Frequently Asked Questions about Bulk Solids Testing
Answers to the most important questions about rheological measurements and bulk solids analysis
Depending on laboratory capacity, results of bulk solids testing are
available approximately two weeks after sample receipt.
Measurements for time consolidation may extend processing time accordingly.
After completion of measurements, we provide results online for you to access, process, and print. Additionally, you receive a cumulative evaluation of results with scatter coefficients, flow function σc(σ1), evaluation of effective friction angle φe(σ), density functions ρ(σ), and wall friction evaluation φw(σ). This allows direct integration of results into your further calculations.
After completion of measurements, we provide results online for you to access, process, and print. Additionally, you receive a cumulative evaluation of results with scatter coefficients, flow function σc(σ1), evaluation of effective friction angle φe(σ), density functions ρ(σ), and wall friction evaluation φw(σ). This allows direct integration of results into your further calculations.
For standard-compliant performance of bulk solids measurements,
sample material should not exceed 2 mm particle size. Larger
particles can impair measurement accuracy and lead to unreliable results. For
special applications or materials with larger particles, please contact us directly
so we can individually assess measurement feasibility.
Depending on the selection of measurements, approximately 1-2 liters
of sample material per specimen is required for a complete bulk solids analysis
for technological silo calculation.
For simple flowability factor measurements, 0.5 liters is already sufficient.
When creating the quote, we provide you with a precise specification of the
sample volume based on the selected measurements and the number of
samples.
Please ensure that the samples have a representative composition of the entire material to guarantee accurate and reliable results. Please do not send us unnecessarily large quantities of material. All delivered material is homogenized during sample preparation and reduced to the required quantity. Unless otherwise specified, the initial moisture content of the material is maintained for the measurements.
Please ensure that the samples have a representative composition of the entire material to guarantee accurate and reliable results. Please do not send us unnecessarily large quantities of material. All delivered material is homogenized during sample preparation and reduced to the required quantity. Unless otherwise specified, the initial moisture content of the material is maintained for the measurements.
For determining reference stresses, approximate specifications are sufficient
for the following points:
- Silo shape: rectangular or round + dimensions/diameter
- Silo shaft height
- Hopper inclination (relative to vertical)
- Hopper height and/or outlet diameter
- Wall material (polished, smooth, rough, etc.)
- Approximate density
To create a technological silo calculation according to DIN EN 1991-4
the following measurements are required:
- Flow function (multiple yield loci at different consolidation stresses)
- Wall friction (wall friction angles and coefficients)
- Bulk and compression density (density change under load)
- Angle of repose
- Optional: Time consolidation (time-dependent flow behavior)
The flowability factor represents a single value at one
consolidation stress for material comparisons.
The flow function shows flow behavior over a larger stress range.
The flow function shows flow behavior over a larger stress range.
For wall friction measurement we need a wall sample according to
drawing from you. Standard materials are available in our laboratory on request.
The wall samples should have the same surface characteristics as the planned silo material.
All measurements are performed on standardized and certified
instruments in our laboratory. The bulk solids measurements for
the yield locus, wall friction, compression density, and time consolidation
are carried out with standardized shear testers according to ASTM D6682. This
ensures reproducible and comparable results.
After performing the measurements, you receive from us a detailed
test report with assessment of the physical flow behavior of the
material. For the existing silo geometry, we identify possible flow problems
and make possible improvement suggestions for prevention. The report contains all
relevant parameters and recommendations for practical application.
After completion of all necessary measurements for technological silo design, a calculation tool for silo geometry design and flow profile estimation is additionally available to you. This enables the calculation of stresses and flow conditions in the silo based on common methods: stresses in filling and emptying state, bridging (critical outlet diameter), limit criterion for mass flow vs. funnel flow, load on the discharge device, etc.
You can set the silo geometry and calculation bases yourself and have them calculated automatically. The results serve as a design aid and estimation of the stresses and flow conditions of the bulk solid in the silo. Please note that some calculation methods are based on generally used empirical foundations and the software does not replace engineering silo calculation.
After completion of all necessary measurements for technological silo design, a calculation tool for silo geometry design and flow profile estimation is additionally available to you. This enables the calculation of stresses and flow conditions in the silo based on common methods: stresses in filling and emptying state, bridging (critical outlet diameter), limit criterion for mass flow vs. funnel flow, load on the discharge device, etc.
You can set the silo geometry and calculation bases yourself and have them calculated automatically. The results serve as a design aid and estimation of the stresses and flow conditions of the bulk solid in the silo. Please note that some calculation methods are based on generally used empirical foundations and the software does not replace engineering silo calculation.
Why SHEAR-TEST for your bulk solids testing?
- ✓ Over 30 years of experience in bulk solids analysis
- ✓ Standard-compliant measurements according to ASTM D6682
- ✓ Fast processing and detailed reports
- ✓ Personal consultation in method selection
- ✓ Confidential treatment of all data